Microwave Assisted-Extraction of Essential Oil from Fresh Basil (Ocium basilicium L.) Leaves
Microwave Assisted-Extraction of Essential Oil from Fresh Basil (Ocium basilicium L.) Leaves
Ditta Kharisma Yolanda Putri
Department of Chemical Engineering, University of Jember, Indonesia 68121
Atiqa Rahmawati
Department of Chemical Engineering, University of Jember, Indonesia 68121
DOI: https://doi.org/10.19184/jobc.v1i1.105
ABSTRACT
In this research, the extraction of essential oil from fresh basil leaves is conducted using solvent-free microwave extraction (SFME) and microwave hydrodistillation (MHD) methods. Several parameters influence the extraction of basil oil using the SFME method: microwave power, the ratio of the mass of raw material to the volume of the distiller (F/D), material size, and the length of the extraction time. Additionally, the components contained in basil oil and changes in oil gland conditions in basil leaves before and after extraction were also evaluated. The optimum condition was obtained as follows: microwave power of 380 W, a ratio of 0.1 g/mL between the mass of raw material and the volume of the distiller (F/D), raw material size of intact (± 3 cm), and an extraction time of 60 min. Moreover, SFME has a shorter extraction time to produce yields than MHD methods. GC-MS analysis of basil oil identified 49 components. This study demonstrates that the SFME method is more effective than the MHD method for extracting basil oil from fresh leaves, based on both the time of extraction and yield.
Keywords: basil oil, essential oil, microwave hydrodistillation, Ocimum basilicum L., solvent-free microwave extraction
REFERENCES
[1] Indonesia, D. A. & IPB. Indonesia’s Essential Oils (in Bahasa Indonesia). (2009).
[2] S., P. Kemangi dan Selasih (in Bahasa Indonesia). (Trubus Agriwidya, 1996).
[3] Abubakar, E. M. M. Antibacterial potential of crude leaf extracts of Eucalyptus camaldulensis against some pathogenic bacteria. African J. Plant Sci. 4, 202–209 (2010).
[4] Nurcahyanti, A., Dewi, L. & Timotius, K. Aktivitas Antioksidan dan Antibakteri Ekstrak Polar dan Non Polar Selasih (O. sanctum L.) (in Bahasa Indonesia). J. Teknol. dan Ind. Pangan 21, (2011).
[5] Sudarsono, D, G., S, W., IA, D. & Purnomo. Tumbuhan Obat II (Hasil Penelitian, Sifat-Sifat, dan Penggunaannya) (in Bahasa Indonesia). (Pusat Studi Obat Tradisional Universitas Gadjah Mada, 2002).
[6] R, Tambun, R.R.H, Purba & H.K, Ginting. Extraction of basil leaves ( Ocimum canum ) oleoresin with ethyl acetate solvent by using soxhletation method. Mater. Sci. Eng. 4–11 (2017). doi:10.1088/1757-899X/237/1/012032
[7] Al Abbasy, D. W., Pathare, N., Al-Sabahi, J. N. & Khan, S. A. Chemical composition and antibacterial activity of essential oil isolated from Omani basil (Ocimum basilicum Linn.). Asian Pacific J. Trop. Dis. 5, 645–649 (2015).
[8] Chenni, M., Abed, D. El, Rakotomanomana, N., Fernandez, X. & Chemat, F. Comparative Study of Essential Oils Extracted from Microwave Extraction. Molecules (2016). doi:10.3390/molecules21010113
[9] Golmakani, M.-T. & Moayyedi, M. Comparison of heat and mass transfer of different microwave-assisted extraction methods of essential oil from Citrus limon (Lisbon variety) peel. Food Sci. Nutr. 3, 506–518 (2015).
[10] Kusuma, H., Altway, A. & Mahfud, M. Solvent-free microwave extraction of essential oil from dried patchouli (Pogostemon cablin Benth) leaves. J. Ind. Eng. Chem. 58, 343–348 (2017).
[11] Kusuma, H. S., Kharisma, D. & Putri, Y. Solvent-Free Microwave Extraction of Essential Oil from Dried Basil (Ocimum basilicum L .) Leaves of Basil Oi. Chem. Chem. Technology 12, 543–548 (2019).
[12] Bale, A. S. & Shinde, N. H. Research Article Microwave Assisted Extraction of Essential Oil From Lemon Leaves. Int. J. Recent Sci. Res. 4, 1414–1417 (2013).
[13] Kusuma, H. S. & Mahfud, M. RSC Advances The extraction of essential oils from patchouli leaves ( Pogostemon cablin Benth ) using a microwave air-hydrodistillation method as a new green technique. RSC Adv. 7, 1336–1347 (2016).
[14] Guenther, E. Essential Oils Volume IVB (in Bahasa Indonesia). (Universitas Indonesia Press, 1990).
[15] Kusuma, H. S. & Mahfud, M. Comparison of conventional and microwave-assisted distillation of essential oil from Pogostemon cablin leaves: Analysis and modelling of heat and mass transfer. J. Appl. Res. Med. Aromat. Plants 4, 55–65 (2017).
[16] Mahfud, M., Putri, D. K. Y., Dewi, I. E. P. & Kusuma, H. S. Extraction of essential oil from cananga (Cananga odorata) using solvent-free microwave extraction: A preliminary study. Rasayan J. Chem. 10, (2017).
[17] Mondello, L. et al. Studies on the essential oil-bearing plants of Bangladesh. Part VIII. Composition of some Ocimum oils O. basilicum L. var. purpurascens; O. sanctum L. green; O. sanctum L. purple; O. americanum L., citral type; O. americanum L., camphor type. Flavour Fragr. J. 17, 335–340 (2002).
[18] Ferhat, M. A., Meklati, B. Y. & Chemat, F. Comparison of different isolation methods of essential oil from Citrus fruits: cold pressing, hydrodistillation and microwave ‘dry’ distillation. Flavour Fragr. J. 22, 494–504 (2007).
Published
21-08-2020
Issue
Vol. 1 Issue 1 (2020): JOBC: Journal of Biobased Chemicals
Pages
1-11
License
Copyright (c) 2022 JOBC: Journal of Biobased Chemicals
How to Cite
-